| ORGANOLEPTIC TEST | | |
| Appearance, shape, size, consistency, color, smell, taste | BDS 6279 | |
| PHYSICO-CHEMICAL AND BIOCHEMICAL TESTS | | |
| Active acidity (рН) | QOP 504-1-FH-26 | |
| Titrable (total acidity) and alkalinity | BDS 5879 | |
| Water content/dry matter | BDS 5312 item2,item2.1 | |
| Fat content (extraction) | BDS 5439 item2 | |
| Protein content (protein, nitrogen) | BDS ISO 1871 | |
| Sugars content (sucrose, lactose, reducing sugars/invert sugar) | BDS 5439 item3 | |
| Carbohydrates content | QOP 504-1-FH-41 | |
| Starch content | Regulation 900/2008 Annex I | |
| Crude cellulose content (fibers) | BDS ISO 5498; BDS ISO 6541 | |
| Ash content | BDS 5313 item3.1 | |
| Ash content - insoluble ash | BDS 5313 item3.3 | |
| Ash alkalinity | BDS 5313 item3.4 | |
| Table salt content /sodium chloride | QOP 504-1-FH-03 | |
| Energy value | чл. 10 от Наредба №23/2009 | |
| Content of ascorbic acid (Vitamin C) | BDS 13374; QOP 504-1-FH-45 | |
| Testing for presence of epihydrin aldehyde through Kreis reaction (Fat rancidity) | QOP 504-1-FH-30 | |
| Determination of peroxide value | BDS 10386 | |
| Benzoic acid content | BDS 1554 item III.15 | |
| Potassium sorbate content (sorbite) | BDS 15487 | |
| Sulfur dioxide content (total and free) | BDS 11709 item1.2;item2 | |
| Aluminum content | QOP 504-1-FH-07 | |
| Arsenic content | QOP 504-1-FH-19; BDS EN 15763 | |
| Iron content | QOP 504-1-FH-02 | |
| Mercury content | BDS EN 15763 | |
| Iodine content | QOP 504-1-FH-46 | |
| Cadmium content | QOP 504-1-FH-17; BDS EN 15763 | |
| Tin content | BDS 9212 | |
| Calcium content | QOP 504-1-FH-21 | |
| Magnesium content | QOP 504-1-FH-52 | |
| Manganese content | QOP 504-1-FH-04 | |
| Copper content | QOP 504-1-FH-18 | |
| Sodium content | QOP 504-1 ICP/MS-02 | |
| Nickel content | QOP 504-1-FH-24 | |
| Lead content | QOP 504-1-FH-16; BDS EN 15763 | |
| Phosphates (phosphorus) content | QOP 504-1-FH-06 | |
| Chromium content | QOP 504-1-FH-25 | |
| Cyanides content | QOP 504-1-FH-53 | |
| Zinc content | QOP 504-1-FH-23 | |
| Aflatoxin В1 content | QOP 504-1-FH-20 | |
| Aflatoxines В1+В2+G1+G2 (total) | QOP 504-1-FH-34 | |
| Aflatoxin M1 content | QOP 504-1-FH-31 | |
| Deoxynivalenol /DON/ content | QOP 504-1-FH-35 | |
| Zearalenone content | QOP 504-1-FH-36 | |
| Ochratoxin content | QOP 504-1-FH-38 | |
| Т2 toxin content | QOP 504-1-FH-39 | |
| Fumonisin content | QOP 504-1-FH-37 | |
| Refractive index | BDS 4018 | |
| Couverture and filling content | BDS 8386 | |
| Nuts content | BDS 9208 | |
| Chocolate and cocoa products fineness | BDS 9378 | |
| Lipolytic activity in chocolate masses | BDS 15527 | |
| Swelling of buscuits | BDS 15221 | |
| Content of pesticide: Chlororganic Phosphororganic Nitrogen and sulfur-containing | BDS EN ISO 15662 | |
| Sweeteners content: | | |
| - acesulfame К | BDS EN 12856; BDS EN 15911 | |
| - saccharine | BDS EN 12856; BDS EN 15911 | |
| - aspartame | BDS EN 12856; BDS EN 15911 | |
| - cyclamate | BDS EN 12857; BDS EN 15911 | |
| Colorings content: | | |
| Yellow: | | |
| - Sunset Yellow | QOP 504-1-IM-HPLC-01 | |
| - tartrazine | QOP 504-1-IM-HPLC-01 | |
| Red: | | |
| - erythrosine | QOP 504-1-IM-HPLC-01 | |
| - azorubine | QOP 504-1-IM-HPLC-01 | |
| - allura red | QOP 504-1-IM-HPLC-01 | |
| - ponceau | QOP 504-1-IM-HPLC-01 | |
| - amaranth | QOP 504-1-IM-HPLC-01 | |
| Blue | | |
| - indigotine | QOP 504-1-IM-HPLC-01 | |
| - Brillian Blue | QOP 504-1-IM-HPLC-01 | |
| - Patent Blue | QOP 504-1-IM-HPLC-01 | |
| Vitamin content: | | |
| - А (retinol) | BDS EN 12823-1;2 | |
| - А (beta-carotine) | BDS EN 12823-1;2 | |
| - В1 (thiamine) | QOP 504-1-IM-LC/MS-02 | |
| - В3 (niacin) | QOP 504-1-IM-LC/MS-02 | |
| - В6 (pyridoxine) | QOP 504-1-IM-LC/MS-02 | |
| - В7 (biotin/vitamin Н) | QOP 504-1-IM-LC/MS-02 | |
| - С (ascorbic acid) | BDS EN 14130 | |
| - D2 (ergocalciferol) | BDS EN 12821 | |
| - D3 (colecalciferol) | BDS EN 12821 | |
| - Е (tocopherols) | BDS EN 12822 | |
| - К (phytomenadione) | BDS EN 14148 | |
| Content of saturated fatty acids | BDS EN ISO 12966-2+BDS EN ISO 5508 | |
| Content of unsaturated fatty acids | BDS EN ISO 12966-2+BDS EN ISO 5508 | |
| Pharmacological substances residues content: | | |
| Antibiotics (Quinolines) – flumequin | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Sulfonamides) - sulfaguanidin | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Sulfonamides) - sulfadiazine | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Sulfonamides) - sulfamerazin | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Sulfonamides) - sulfamethoxazole | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Sulfonamides) - sulfapyridine | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Sulfonamides) - sulfatiazol | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Sulfonamides) - sulfacetamide | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Tetracyclines) – oxytetracycline хидрохлорид | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Tetracyclines) – tetracycline hydrochloride | QOP 504-1-IM-LC/MS-01 | |
| Antibiotics (Tetracyclines) – chlortetracycline hydrochloride | QOP 504-1-IM-LC/MS-01 | |
| MICROBIOLOGICAL TESTS | | |
| Total number of microorganisms, including mesophilic aerobes and facultative anaerobes | BDS ЕN ISO 4833-1 BDS ЕN ISO 4833-2; BDS 12334 item5, item10 | |
| Bacillus species including Bacillus Cereus | BDS EN ISO 21871 item9.1; item9.2; BDS EN ISO 7932 | |
| Bacillus species including Bacillus subtilis (var. mesentericus) | BDS EN ISO 21871 item9.1; item9.2; BDS EN ISO 7932 | |
| Water activity | ISO 21807 | |
| Yeast | BDS ISO 21527-1; -2; BDS 12334 item11 | |
| Escherichia coli | ISO 16649-2; ISO 7251 item9.1; item9.2 | |
| Escherichia coli O157 | BDS EN ISO 16654 | |
| Enterobacteria, including Proteus, Klebsiella, Citrobacter | ISO 21528-1 item9.2; item9.3; ISO 21528-2 | |
| Yersinia enterocolitica | BDS EN ISO 10273 | |
| Clostridia sulfite-reducing | ISO 15213 | |
| Coagulase-positive staphylococci | BDS EN ISO 6888-1+A1;-2+A1;-3+AC item9.1;-3+AC item9.2; BDS 12334 item8 | |
| Coliforms | ISO 4831item9.1; item9.2; ISO 4832 | |
| Leuconostoc | COMECON ST 5806 | |
| Lipolytic microorganisms | BDS 12334 item7 | |
| Listeria monocytogenes | BDS EN ISO 11290-1+А1; -2+А1 | |
| Mesophilic lactic bacteria | BDS ISO 15214 | |
| Moulds | BDS ISO 21527-1;-2; BDS 12334 item11 | |
| Pseudomonas aeruginosa | BDS EN ISO 13720 | |
| Psychrotrophic microorganisms | BDS ISO 17410 | |
| Salmonella species | BDS ЕN ISO 6579; SD СЕN ISO/ TS 6579-2 | |
| Shigella species | BDS EN ISO 21567 | |
| Genetically modified organisms | | |
| Determination of presence of genetically modified organisms – 35S | BDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1 | |
| Determination of presence of genetically modified organisms – FMV | BDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1 | |
| Determination of presence of genetically modified organisms – NOS terminator | BDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1 | |
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| 23 Crystal sugar | | |
| ORGANOLEPTIC TEST | | |
| Taste, smell, solubility in water, foreign impurities | BDS 391, item11 | |
| PHYSICO-CHEMICAL AND BIOCHEMICAL TESTS | | |
| Active acidity (рН) | QOP 504-1-FH-26 | |
| Titrable (free acidity) | QOP 504-1-FH-12 | |
| Water content/dry matter | BDS 391 item4 | |
| Sugars content (sucrose, reducing sugars/invert sugar, polarization) | BDS 391 item5;item6; Наредба за изискванията към захарите, предназначени за консумация от човека Приложение 6; Приложение 11 | |
| Carbohydrates content | QOP 504-1-FH-41 | |
| Crude cellulose content (fibers) | BDS ISO 5498; BDS ISO 6541 | |
| Ash content | BDS 391 item7; Наредба за изискванията към захарите, предназначени за консумация от човека; Приложение 1, Раздел1 | |
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| Sulphated ash content | Наредба за изискванията към захарите, предназначени за консумация от човека; Приложение 5 | |
| Table salt content /sodium chloride | QOP 504-1-FH-03 | |
| Energy value | чл. 10 от Наредба №23/2009 | |
| Content of ascorbic acid (Vitamin C) | QOP 504-1-FH-45 | |
| Starch content – quality response | QOP 504-1-FH-28 | |
| Benzoic acid content | BDS 1554 item III.15 | |
| Potassium sorbate content | BDS 11712 item2 | |
| Soy protein content | QOP 504-1-FH-32 | |
| Aluminum content | QOP 504-1-FH-07 | |
| Antimony content | QOP 504-1 ICP/MS-04 | |
| Arsenic content | QOP 504-1-FH-19; BDS EN 15763 | |
| Barium content | BDS EN ISO 17294-2 | |
| Boron content | BDS EN ISO 17294-2 | |
| Iron impurities content | BDS 391 item10 | |
| Mercury content | BDS EN 15763 | |
| Iodine content | BDS EN 15111 | |
| Cadmium content | QOP 504-1-FH-17; BDS EN 15763 | |
| Tin content | QOP 504-1-FH- 57; BDS EN 15765 | |
| Calcium content | QOP 504-1-FH-21 | |
| Magnesium content | QOP 504-1-FH-52 | |
| Manganese content | QOP 504-1-FH-04 | |
| Copper content | QOP 504-1-FH-18 | |
| Sodium content | QOP 504-1 ICP/MS-02 | |
| Nickel content | QOP 504-1-FH-24 | |
| Lead content | QOP 504-1-FH-16; BDS EN 15763 | |
| Selenium content | BDS EN ISO 17294 | |
| Sulphates content | QOP 504-1-FH-09 | |
| Phosphates (phosphorus) content | QOP 504-1-FH-06 | |
| Chromium content | QOP 504-1-FH-25 | |
| Cyanides content | QOP 504-1-FH-53 | |
| Zinc content | QOP 504-1-FH-23 | |
| Determination of solution color (ICUMSA method) | Наредба за изискванията към захарите;Приложение 1, itemIII | |
| Potassium content | QOP 504-1 ICP/MS-01 | |
| Content of pesticide: Chlororganic Phosphororganic Nitrogen and sulfur-containing | BDS EN ISO 15662 | |
| Sweeteners content: | | |
| - acesulfame К | BDS EN 12856; BDS EN 15911 | |
| - saccharine | BDS EN 12856; BDS EN 15911 | |
| - aspartame | BDS EN 12856; BDS EN 15911 | |
| - cyclamate | BDS EN 12857; BDS EN 15911 | |
| MICROBIOLOGICAL TESTS | | |
| Total number of microorganisms, including mesophilic aerobes and facultative anaerobes | BDS ЕN ISO 4833-1; BDS ЕN ISO 4833-2 | |
| Bacillus species | BDS EN ISO 21871 item9.1; item9.2; BDS EN ISO 7932 | |
| Water activity | ISO 21807 | |
| Yeast | BDS ISO 21527-1; -2 | |
| Escherichia coli | ISO 16649-2; ISO 7251 item9.1; item9.2 | |
| Enterobacteria, including Proteus, Klebsiella, Citrobacter | ISO 21528-1 item9.2; item9.3;ISO 21528-2 | |
| Clostridia Sulfite-reducing | ISO 15213 | |
| Coagulase-positive staphylococci | BDS EN ISO 6888-1+A1; -2+A1; -3+AC item9.1; item9.2 | |
| Coliforms | ISO 4831 item9.1; item9.2; ISO 4832 | |
| Leuconostoc | COMECON ST 5806 | |
| Lipolytic microorganisms | BDS 12334 item7 | |
| Listeria monocytogenes | BDS EN ISO 11290-1+А1; -2+А1 | |
| Moulds | BDS ISO 21527-1; -2 | |
| Pseudomonas aeruginosa | BDS EN ISO 13720 | |
| Psychrotrophic microorganisms | BDS ISO 17410 | |
| Salmonella species | BDS ЕN ISO 6579; SD СЕN ISO/TS 6579-2 | |
| Streptococci | BDS 14593 item6.9 | |
| Shigella species | BDS EN ISO 21567 | |
| GENETICALLY MODIFIED ORGANISMS | | |
| Determination of presence of genetically modified organisms – 35S | BDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1 | |
| Determination of presence of genetically modified organisms – FMV | BDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1 | |
| Determination of presence of genetically modified organisms – NOS terminator | BDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1 | |